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PQ Index When wear occurs in equipment, the particles resulting from the wear process can be of several types, namely: Normal Wear - small wear particles due to typical welding/breaking cycle as outlined in earlier discussions. Significant wear - medium sized particles causing gouging of metal and resulting in larger than normal particles being generated. These in turn become the cause of even larger particle generation. Severe Wear - large particle occurrence which may reflect presence of metal particles due to fatigue fracture or pitting of the metal components. This production of large metal chips can in turn induce enough wear to cause further disintegration and rapid onset of failure. Since most of the metal fragments referred to in the above wear scenarios are iron in nature, the effect of the particles on a magnetic field can be used to detect the type of wear. Small fragments would, as expected, have the least effect on a magnetic field, while the large chips of iron would be expected to have a large effect. The instrument used in the laboratory for determination of Particle Quality (PQ), measures the effect of the wear particles on a magnetic field. When calibrated on known standards, an index or relationship number can be produced and from this the criteria for satisfactory, significant and severe wear can be determined and reported as the PQ Index. Dispersancy Dispersant additives are incorporated in engine oil formulations to ensure that minimal accumulation of contaminants that result in sludging will occur. Sludging is the combination of mainly moisture and soot or wear debris from the engine. It can adversely affect the engine operation through filter plugging, deposition on moving surfaces and by thickening of the oil to an extent that incorrect lubricant supply will result. RULER measurement of Anti-Oxidant Content
Glycol by gas chromatography method Glycol contamination in an engine due to coolant leakage is a major problem and requires accurate and reproducible assessment. One method is by a process called Head Space Gas Chromatographic Analysis. A sample of engine oil is heated above the boiling point of glycol (180-200oC) and the vapours collected are measured by gas chromatography. Another method by Fourier Transform Infra-Red (FTIR) analysis is unreliable and subject too many interferences from oxidation products in the oil as well as moisture.
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